GB∕T 38171-2019 金属螯合层析介质

书书书G21G22G21G22G23G24G25ＧＢ／Ｔ１．１—２００９G26G27G28G29G2AG2BG2C。G21G22G23G2DG2EG2FG22G23G30G31G32G33G34G27G35G36G37。G21G22G23G2BG2CG38G39：G2EG2FG3AG3BG33G3CG3DG3EG3DG31G32G3F、G2EG2FG22G23G30G31G32G33、G2EG3AG40G41G42G43G44G45（G46G47）G48G49G4AG4B。G21G22G23G4CG4DG2BG2CG4E：G4FG50G51、G52G53、G54G55、G56G3BG57、G58G59G41、G46G5AG2F、G5BG5CG5D、G58G5EG5F、G60G61G62、G63G64G65。Ⅰ犌犅／犜３８１７１—２０１９G23G24G25G26G27G28G29G2A１ G2BG2CG21G22G23G29G66G67G68G69G6AG6BG6CG6DG6EG6FG28G70G71、G44G45G4DG72、G73G74G5CG75、G73G76G29G2A、G22G77、G22G5A、G78G79、G7AG7BG7CG7DG7E。G21G22G23G7FG80G81G68G69G6AG6BG6CG6DG6EG6FG28G82G83G84G73G74。２ G2DG2BG2EG2FG30G31G32G85G86G87G88G89G81G21G87G88G28G8AG80G8BG8CG8DG8EG64G28。G8FG8BG90G91G92G28G93G80G87G88，G94G90G91G92G28G95G21G7FG80G81G21G87G88。G8FG8BG8DG90G91G92G28G93G80G87G88，G96G97G98G95G21（G78G99G3FG48G28G9AG9BG38）G7FG80G81G21G87G88。ＧＢ／Ｔ１９１ G78G79G9CG7AG9DG9EG22G5AＧＢ／Ｔ５４７５ G9FGA0GA1GA2GA3GA4GA5GA6G5CG75ＧＢ／Ｔ６６８２ G70G6DGA7G76GA8G80GA9G29GAAG7CGABG76G5CG75G2EGACG4EGADGAEG7CG2FGAFGB0（２０１５GB1G95）３ G33G34G35G36G37G85G86G45GB2G7CG66GB3G7FG80G81G21G87G88。３．１G23G24G25G26G27G28G29G2A犿犲狋犪犾犮犺犲犾犪狋犻狀犵犮犺狉狅犿犪狋狅犵狉犪狆犺犻犮犿犲犱犻狌犿GB4GB5GB6GB7GB8GB9GBAGBBGBCGBDGBEGB7GBFGB9GBAGC0G6BGC1GC2GA4GC3G70G9FG6EG6FGC4，GC5G6AG6BG68G69G9FGA0Ｎｉ２＋（GBBG96GC6G68G69G9FGA0）GC7GC8GC9G28GCAG71G6CG6DG6EG6F。４ G38G39G24G6AG6BGCBGCCG71G70GCDGB5GB6GB7GB8GB9GBAGCEG68G69G6AG6BG6CG6DG6EG6F（ＩＤＡ）G7CGBDGBEGB7GBFGB9GBAGCEG68G69G6AG6BG6CG6DG6EG6F（ＮＴＡ）。５ G3AG33G3BG3C５．１ G3DG3EG3BG3CG68G69G6AG6BG6CG6DG6EG6FG8AG43GC8GCFGD0、GD1GD2G59GD3，GC1G59G3BGD4G42GD5G85G8AGD6G48GD7GD8GD9。５．２ G2EG3FG3BG3CG8AGDAG6BGD1１G2EG28G29G66。１犌犅／犜３８１７１—２０１９G40１ G23G24G25G26G27G28G29G2AG41G42G3BG2EG3FG3BG3CGDBGDCGDDG22ＩＤＡＮＴＡGDEGDFGE0GE1GDEGDFGE2（犠GDEGDF）／％≥９０ａGE3GE4GDEGDF（犱）／μｍ９０．０±１３．５G97GE5GE6GE7ｂ／（ｃｍ／ｈ）≥２７０GE8GB7GE9GEAｃ／（μｍｏｌ／ｍＬ）≥３６．００≥１５．００GEBGECGEDGEE（犙５０％）ｄ／（ｍｇ／ｍＬ）≥４０．００GEFGF0GF1GF2／（ＣＦＵ／ｍＬ）＜１００５GF3GF4GB7GF5GF6GF7GF0GEE／（μｇ／ｍＬ）ｐＨ３．０≤０．１６≤０．３５ｐＨ１３．０≤０．１０≤０．１５ａGDEGDFGC1４５．０μｍ～１６５．０μｍGE0GE1GF8GABGA6GF9GDEG28GFAGFBG84GFCGFDGABGA6GF9GDEGFAGFBGFEGE2。ｂGC1０．１０ＭＰａGFFG21G85G8EG22G97GE5GE6GE7。ｃG23G24G25G6EG6FG89Ｎｉ２＋G28G6AG6BGEE。ｄG23G24G25G6EG6FG89G26GBAGF7G27G28（ＨｉｓｔａｇｇｅｄＬＤＨ）G28G29G2AGEE。６ G43G44G45G46６．１ G3DG3E６．１．１ G47G48G49G4AG24G25ＧＢ／Ｔ５４７５G2BG2CG2DG83G2EG2EG2FGA5５ｍＬGA6G2E，G30G81５０ｍＬＧ３GCEG31G32G33G34G35G2EG2FG36５ｍｉｎ。G80GDAG6BＧＢ／Ｔ６６８２G28GBFG37GA9G38G39５GBD，G23GBD２ｍｉｎ，G97G3AG80G3BG3CG3DGC1０．１ＭＰａGFFG21G85G2FG36５ｍｉｎ。GB4G39G3EG28G68G69G6AG6BG6CG6DG6EG6FG30G81G3FG40G2E，G41G96G2EG42G43GBFG37GA9，G44G45G68G69G6AG6BG6CG6DG6EG6FGC4G8AG48２ｃｍG28GBFG37GA9。G46G47G3AG48G49G68G69G6AG6BG6CG6DG6EG6FG84GA9G28G46G6BGFAG4A。６．１．２ G47G48G3EG44G80G4BG4CG29G4DG29GA5G46G6BGFAG4AG30G81GEDG4EG4FGC4，G50G51GD4G42GD5G52G53G54GF2。G55G56G57G58８０％G55GC4GD2GFBGE4GCDG68G69G6AG6BG6CG6DG6EG6FGCDG22G23，G80G4BG4CG29G4DG59G5AGEDG4EG4FGC4G28G68G69G6AG6BG6CG6DG6EG6F，G97G3AG80G5BG4EG4FGFFGC4。G50G5CG59G3BGD4G42GD5G5DG5E，G5FG56G57G2EG28G60G61G38G62。G63G64G68G69G6AG6BG6CG6DG6EG6FG25G4FG35G44G7E。６．２ G4BG4C６．２．１ G47G48G49G4AG5CG75G65６．１．１。６．２．２ G47G48G43G44G66G30G67G59GDEGEAG68G69GF2G6AG85：G74GEEGF9GDEG71GCEGCDG6BG80GCE，G70G6CGCBG71GCEGCDGA9，G70G6DG6DG6EGCDG38G6FG6DG6E，G70G43GA6G2EG5FG71G74G66。２犌犅／犜３８１７１—２０１９６．２．３ G4DG4EG4FG50６．２．３．１ G2BG2CG4BG4CG51G24G6E（１）G72G73：犠GDEGDF＝∑１６５犽＝４５犠犽…………………………（１）G6EG2E：犠GDEGDF———GE0GE1GDEGDFGE2，％；犠犽———GDEGDFGCD犽（μｍ）GF9GDEG28GFAGFBG84GFCGFDGABGA6GF9GDEGFAGFBGFEGE2，％。６．２．３．２ G52G53G4BG4CG24G6E（２）G72G73：犱＝∑狀犽＝１犱犽犖…………………………（２）G6EG2E：犱———G3FG74G72G28GCAG66GF2GEEG6EG6FGF9GDEG28GE3GE4GDEGDF，G38G39GCDG42G75（μｍ）；犱犽———G38G76GF9GDEG28GDEGDF，G38G39GCDG42G75（μｍ）；犖———G3FG74G72G28G6EG6FGF9GDEG28GF2GDC。GC1G77G78GD9G79G88G85G7AG48G28GBFGBDG7BG7CG74G66G7DG7EG28G7FG89G80G81G8DG48G82G3CG73G45GE3GE4G81G28１０％。６．３ G54G55G56G57６．３．１ G47G48G49G4AG5CG75G65６．１．１。６．３．２ G47G48G58G59G83G80１．６０ｃｍ×２０．００ｃｍG28G6CG6DG84，G85G86G84GA0G27G37，GB4G6EG6FG84GA9G28G46G6BG87G88G89G8AG6CG6DG84G2E，G8BG30，G8CG8DG6EG6FG8EG6CGE5GEAGCD１０．００ｃｍ±０．２０ｃｍ，G84GA0GC4G8FG90GD0GA9。G91G92G84GA0G8AG37，G55０．５ｍＬ／ｍｉｎG28GE6GE7G93G94G41G84G2EG6BG8A１０G76G84GFAGFBG28GBFG37GA9，G8EG6CG95G66G3AG96G8EG5FG71G74GAB。６．３．３ G47G48G44G36GB4G6CG6DG84G93G8AG2EG97GFFG6CG6DG4AG74。G74G66G98，G2DG99G92G9AG66G66GCAG66GE6GE7狏狓（ｍＬ／ｍｉｎ），G44G9BG9CGE6GE7５ｍｉｎG3A，G9DG9EG9FG98G84GFF狆狓（ＭＰａ）。GA0G94G59G43GE6GE7，G35G74G66GA1G8AGE6GE7G85G28G84GFF。G2BG49GFFG21G22G49０．１０ＭＰａGCDGA2，G9FG98G89G8AGE6GE7G9DG9EGCD狏０．１。６．３．４ G4DG4EG4FG50G24G6E（３）G72G73：犉ｍａｘ＝６０狏０．１犛…………………………（３）G6EG2E：犉ｍａｘ———G97GE5GE6GE7，G38G39GCDGA3G75G23GA4G98（ｃｍ／ｈ）；狏０．１———GC1０．１０ＭＰａGFFG21G85G28GFAGFBGE6GE7，G38G39GCDG24G25G23G70（ｍＬ／ｍｉｎ）；３犌犅／犜３８１７１—２０１９犛———G6CG6DG84GA5GD2GFB，G38G39GCDGE3G5CGA3G75（ｃｍ２）；６０———G70GA6GA7G30GCDGA4G98G28GA2G73G4AGF2。GC1G77G78GD9G79G88G85G7AG48G28GBFGBDG7BG7CG74G66G7DG7EG28G7FG89G80G81G8DG48G82G3CG73G45GE3GE4G81G28１０％。６．４ G5AG5BG5CG5D６．４．１ G5EG5FG5AG60６．４．１．１ G61G62G63G64G65G66G5FG67，狆犎１０．０GB4GA8G30GA9６８．００ｇGAAG81３００ｍＬGBFG37GA9G2E，G43GABGB6GA9５７０ｍＬ，G80GBFG37GA9GACGAD，G50ｐＨGCD１０．０，G97G3AG66GAEGAF１０００ｍＬ。６．４．１．２ G61G62G63G64G65G66G5FG68，狆犎１０．０GB0GA5GA8G30GA9５．４０ｇ，G43GBFG37GA9５０ｍＬGAAGB1G3A，G43３５ｍＬGABGB6GA9，G80GBFG37GA9GACGAD，G50ｐＨGCD１０．０，G97G3AG66GAEGAF１００ｍＬ。６．４．１．３ ５犵／犔G69G6A犜G6BG6CG5FGB0GA5０．５０ｇGB2GB3ＴG43GB4GBAGF3GB5４．００ｇGAAG81１００ｍＬGB9GB6G2E。６．４．１．４ G6DG6EG6FG70G6BG6CG71GB0GA5GB7GB8GBAGB5１．００ｇ，G43GA8G30GB9１００．００ｇG81G31GBAGF8G31GC9GBBGBC，G79G8AGBDGBEG36G3EG28GBFG37GC0G2EGC1G80。６．４．１．５ ０．１０犿狅犾／犔G68G72G70G73G68G6FG72G74（G75G76犈犇犜犃G77G78G5EG5F）GB0GA5４０．００ｇGB9GB8GB5GC2GB9GBAGB8GB9，GAAG81１０００ｍＬGBFG37GA9G2E，GC3GC4，GC5G47。６．４．１．６ ０．１０犿狅犾／犔犈犇犜犃G77G78G5EG5FG41G77G36GB0GA5０．２５００ｇG81８００℃GC6G3FGAFGC7G77G28GB7G23GC8G30GC9，GB0G23GAF０．０００１ｇ。G80G64GEEGBFG37GA9GCAGCB，G43５ｍＬ２０％G28GB4GBAGAAG88G5FGA6G2EGAAGB1，G43１０ｍＬGBFG37GA9，G80１０％GB6GA9GAAG88G2EG7CGAFｐＨ７～８，G43１０ｍＬGB6GA8G30GA9GCCGCDG88GF4（ｐＨ１０）GCE５GCF５ｇ／ＬGB2GB3ＴGDDG9EG88，G80GE8G8DGD0G28ＥＤＴＡG22G23GAAG88GCFG66GAFGAAG88G2DGB7GBEGD1GCDGD2GD3GBE。G65G98GD4G3CGD5GABG76。６．４．１．７ 犈犇犜犃G77G78G5EG5FG79G5DG4FG50G24G6E（４）G72G73：犮ＥＤＴＡ＝犿（犞１－犞２）×０．０８１３８…………………………（４）G6EG2E：犮ＥＤＴＡ ———GB9GB8GB5GC2GB9GBAGB8GB9G22G23GAAG88G28GABGEA，G38G39GCDGD6GD7G23G25（ｍｏｌ／Ｌ）；犿———GC8G30GC9G6FGEE，G38G39GCDGD8（ｇ）；犞１———GB9GB8GB5GC2GB9GBAGB8GB9GAAG88G80GEE，G38G39GCDG24G25（ｍＬ）；犞２———G3CGD5GABG76G80GB9GB8GB5GC2GB9GBAGB8GB9G80GEE，G38G39GCDG24G25（ｍＬ）；０．０８１３８———１．００ｍＬGB9GB8GB5GC2GB9GBAGB8GB9G22G23GAAG88GA7G30GCDGA1GD9G6FGEEGC8G30GC9G28GA2G73G4AGF2。６．４．１．８ ０．０５犿狅犾／犔犖犻（犖犗３）２G77G78G5EG5FGB0GA5１．４５ｇＮｉ（ＮＯ３）２·６Ｈ２ＯGAAG81１００ｍＬGBFG37GA9G2E。４犌犅／犜３８１７１—２０１９６．４．１．９ ０．０５犿狅犾／犔犖犻（犖犗３）２G77G78G5EG5FG41G77G36G23GDAGEEGA5５０ｍＬGC4GDBGE8G8DG28Ｎｉ（ＮＯ３）２GAAG88G30G81２５０ｍＬGBFGDCGC0G2E，G80GB6GA9G50G5CｐＨG81GAF７～８，G43G8A５０ｍＬGB6GA8G30GA9GCCGCDG88GB9，０．２５ｇGB7GB8GBAGB5GDDG9EGCB，G80０．１ｍｏｌ／ＬG28ＥＤＴＡG22G23GAAG88G5FG71GCFG66GAFGAAG88G2DG4FGBEGD1GCDGB7GBEGCDGDDGDE。G9DG9EG3FGDFGE0G28ＥＤＴＡG22G23GAAG88G28GFAGFB犞ＥＤＴＡ，０。６．４．２ G47G48G49G4AG24G25ＧＢ／Ｔ５４７５G2BG2CG2DG83G2EG2EG2FGA5５ｍＬGA6G2E，G30G81５０ｍＬＧ３GCEG31G32G33G34G35G2E。G80GBFG37GA9G38G39５GBD，G23GBD２ｍｉｎ，GC5G80０．１ｍｏｌ／ＬＥＤＴＡGAAG88G38G39５GBD，G23GBD５ｍｉｎ，GB4G6EG6FGC4G6AG6BG28G68G69G9FGA0G38G39G3E，G97G3AG80GBFG37GA9G38G39５GBD，G23GBD２ｍｉｎ，G3BG3CG3DGC1０．１ＭＰａGFFG21G85G2FG36５ｍｉｎ。６．４．３ G47G48G58G59GB0GA5２．００ｇG2FG36G28G6EG6F，GB4G96G84GA9G28G46G6BG87G88G89G8AG6CG6DG84G2E，G85G86G84GA0G27G37，G8BG30，GE1G84G8EG6CG95G66。G91G92G84GA0G8AG37，G93G94G41G84G2EG6BG8AGBFG37GA9（１０G76G84GFAGFB），G44G9BG8EG6CG95G66。６．４．４ G47G48G44G36G23GDAGEEGA5５０ｍＬＮｉ（ＮＯ３）２G22G23GAAG88，G47GE7G6BG3CG84GF8，G7CG96GE2GE3GE6G27G88；GC5G80５０ｍＬGBFG37GA9G39GE4，G65G98GE2GE3GE6G27G88，GB4G3FG48GE2GE3G28GE6G27G88G46G6B。GC4GDBGE2GE3G28Ｎｉ（ＮＯ３）２GE6G27G88G80GB6GA9G50G5CｐＨG81GAF７～８，G43G8A５０ｍＬGB6GA8G30GA9GCCGCDG88GB9，０．２５ｇGB7GB8GBAGB5GDDG9EGCB，G80０．１ｍｏｌ／ＬG28ＥＤＴＡG22G23GAAG88G5FG71GCFG66GAFGAAG88G2DG4FGBEGD1GCDGB7GBEGCDGDDGDE。G9DG9EG3FGDFGE0G28ＥＤＴＡG22G23GAAG88G28GFAGFB犞ＥＤＴＡ，１。６．４．５ G4DG4EG4FG50GE5GE6G6E（５）G72G73：ρＮｉ２＋＝犮ＥＤＴＡ（犞ＥＤＴＡ，０－犞ＥＤＴＡ，１）犿×１．４×１０００…………………………（５）G6EG2E：ρＮｉ２＋ ———G68G69G6AG6BG6CG6DG6EG6FGE8GB7GE9GEA，G38G39GCDG42GD6GD7G23G24G25（μｍｏｌ／ｍＬ）；犮ＥＤＴＡ———ＥＤＴＡG22G23GAAG88GABGEA，G38G39GCDGD6GD7G23G25（ｍｏｌ／Ｌ）；犞ＥＤＴＡ，０———Ｎｉ（ＮＯ３）２G22G23GAAG88GDFGE0ＥＤＴＡG22G23GAAG88GFAGFB，G38G39GCDG24G25（ｍＬ）；犞ＥＤＴＡ，１———GE2GE3G49G28Ｎｉ（ＮＯ３）２GE6G27G88GDFGE0ＥＤＴＡG22G23GAAG88GFAGFB，G38G39GCDG24G75（ｍＬ）；犿———G68G69G6AG6BG6CG6DG6EG6FG6FGEE，G38G39GCDGD8（ｇ）；１．４———G68G69G6AG6BG6CG6DG6EG6FG6FGEEGA7G30GCDGFAGFBG28GA2G73G4AGF2。GC1G77G78GD9G79G88G85G7AG48G28GBFGBDG7BG7CG74G66G7DG7EG28G7FG89G80G81G8DG48G82G3CG73G45GE3GE4G81G28１０％。６．５ G7AG7BG7CG7D６．５．１ G5EG5FG5AG60６．５．１．１ G65G66G5F犃，狆犎７．４G23GDAGB0GA5５．８０ｇＮａ２ＨＰＯ４·１２Ｈ２Ｏ、０．５９ｇＮａＨ２ＰＯ４·２Ｈ２Ｏ、５．８４ｇＮａＣｌG7C３．４０ｇGE7GE8，G80GBFG37GA9GAAGB1，G50G5CｐＨGAF７．４，GC5G66GAEGAF１０００ｍＬ，G97G3AG80０．４５μｍGE9GDFG28GEAGEBG3CGEA。６．５．１．２ G65G66G5F犅，狆犎７．４G23GDAGB0GA5２．９０ｇＮａ２ＨＰＯ４·１２Ｈ２Ｏ、０．２９ｇＮａＨ２ＰＯ４·２Ｈ２Ｏ、２．９２ｇＮａＣｌG7C１７．０２ｇGE7GE8，G80GBF５犌犅／犜３８１７１—２０１９G37GA9GAAGB1，G50G5CｐＨGAF７．４，GC5G66GAEGAF５００ｍＬ，G97G3AG80０．４５μｍGE9GDFG28GEAGEBG3CGEA。６．５．１．３ 犎犻狊狋犪犵犵犲犱犔犇犎G47G48（G7EG5D＞９５％）GB0GA5３００．０ｍｇＨｉｓｔａｇｇｅｄＬＤＨGECG36GBB（G80GB8G37GA9GD7G6DG3AGECG36，GD2GEA＞９５％），GAAGB1G81１００ｍＬGCCGCDG88ＡG2E，GABGEAGCD３．０ｍｇ／ｍＬ，G24G25《G2EGACG4EGADGAEG7CG2FGAFGB0》（２０１５GB1G95）（０７３１）GEDG58GEEGEFGD3G75G22G66GF0GD5GABGEA，GC5G80０．４５μｍGE9GDFG28GEAGEBG3CGEA。６．５．１．４ １％（G7FG80G38G81）G82G83G5EG5FG23GDAGEEGA5０．１ｍＬGF1GF2，G43GBFG37GA9G46G6B，G66GAEGAF１０ｍＬ。６．５．２ G47G48G49G4AG5CG75G65６．１．１。６．５．３ G47G48G58G59G83G80１．６０ｃｍ×２０．００ｃｍG28G6CG6DG84，G85G86G84GA0G27G37，GB4G6EG6FG84GA9G28G46G6BG87G88G89G8AG6CG6DG84G2E，G8BG30，G8CG8DG6EG6FG8EG6CGE5GEAGCD５．００ｃｍ±０．２０ｃｍ，G84GA0GC4G8FG90GD0GA9。G91G92G84GA0G8AG37，G55２．０ｍＬ／ｍｉｎG28GE6GE7G93G94G41G84G2EG6BG8A１０G76G84GFAGFBG28GBFG37GA9，G8EG6CG95G66G3AG96G8EG5FG71G74GAB。６．５．４ G47G48G44G36GB4G6CG6DG84G93GC1G6CG6DG4AG74G2E，G35G73G74２８０ｎｍGF3GB7GF4GF5（ＵＶ）GF6G31，G89GEDGEEG74G66G3CG3DG5FG71GF7G8C。GEBGECG7DG6BGEDGEEG80５０％GF8GD7G81GD1G9E。G74GEEG35G9DG9EGA6G2EＨｉｓｔａｇｇｅｄＬＤＨG28１００％ＵＶGF6G31，G78G99G8DG7DG6BG49G6EG6FGC4G28ＨｉｓｔａｇｇｅｄＬＤＨG28GB7GF4G29GE2。G80GCCGCDG88ＡG55２．０ｍＬ／ｍｉｎGE6GE7GE3GF9G6CG6DG84GAFGB7GF4GB7GF5GE3GF9，G55２．０ｍＬ／ｍｉｎGE6GE7GC4GA6，GE1GE6GF8GFAGF5G2EＨｉｓｔａｇｇｅｄＬＤＨG28ＵＶGF6G31GABGEAGCD５０％G28GA6G2EGABGEAG98GC4GA6G7DGFB，G9DG9EGC4GA6GFAGFB。GC4GA6G7DGFBG3AG80GCCGCDG88ＡG55２．０ｍＬ／ｍｉｎG28GE6GE7GE3GF9GB7GF4GF6G31GAFGB7GF5；G80GCCGCDG88ＢG55２．０ｍＬ／ｍｉｎG28GE6GE7G5FG71G39GF7。G72G73GEBGECGEDGEE。GFCG44GFDG79G88G85GF8GD7GFAGFBG74G66：GB4G6CG6DG84G93GC1G6CG6DG4AG74G2E，G35G73G74２８０ｎｍGF3ＵＶGF6G31，GC4GA6１０μＬ１％GF1GF2，G9DG9EG85G27GFEＵＶGF6G31G97G53G98G89G8AG28GFAGFB。６．５．５ G4DG4EG40G6CG24G6E（６）G72G73：犙５０％＝犆０（犞１－犞０）犞ｇｅｌ…………………………（６）G6EG2E：犙５０％———G6EG6FG28GEBGECGEDGEE，G38G39GCDG24GD8G23G24G25（ｍｇ／ｍＬ）；犆０———GF0GD5G2BG9AGABGEA，G38G39GCDG24GD8G23G24G25（ｍｇ／ｍＬ）；犞１———G84G27G37GF0GD5GABGEA犆G22G49G8AG37GF0GD5GABGEA犆０G28５０％G98GE6G27G88GFAGFB，G38G39GCDG24G25（ｍＬ）；犞０———GFCG44GFDG79G88G85GF8GD7GFAGFB，G38G39GCDG24G25（ｍＬ）；犞ｇｅｌ———G6EG6FGFAGFB，G38G39GCDG24G25（ｍＬ）。GC1G77G78GD9G79G88G85G7AG48G28GBFGBDG7BG7CG74G66G7DG7EG28G7FG89G80G81G8DG48G82G3CG73G45GE3GE4G81G28１０％。６．６ G84G85G86G81６．６．１ G47G48G21G49G4AG5CG75G65６．１．１。６犌犅／犜３８１７１—２０１９６．６．２ G47G48G44G36G69G25《G2EGACG4EGADGAEG7CG2FGAFGB0》（２０１５GB1G95）（１１０５）GFCGFFGEFG83G2EG42G82G21G49GEAG73G22———G42G82G21G72GF2G75G5FG71。GA5１ｍＬG2FG36G6EG6F，G43G8A１ｍＬGBFG37GA9，G23G80G24G25G46G6BG26G46G47GA6G2E。GB4G27G48３０ｍＬG28GF0GD5G29G53G2AGC2GA4G2BG2CGB7G28G2DGC8GC0１２１．０℃G2EGEF２０ｍｉｎ，G52G8A４０．０℃GC7G2FG30G2E，GE1G2BG2CGB7GC3GC4G49４０．０℃G98，G80G42GEEG31G88G26G29GA5１ｍＬG46G47G3AG28GA6G2EG43G8AG9CG2DGC8GC0G2E，G46G47，G32G46G6BG21G89G8AG2BG2CG33G2E，G5BGD0GC4G5B。GC1GA8G2FG85G5FG46G6BG21G34G35。G32G2BG2CG33G30G81GC7G2FG30G2E３５．０℃G36G37５ｄ。６．６．３ G4DG4EG4FG50G36G37G92G3AG73G22G2BG2CG33。G72GF2GEFGF0GC8GC9G38G39GF2（ＣＦＵ）。GC1G77G78GD9G79G88G85G7AG48G28GBFGBDG7BG7CG74G66G7DG7EG28G8DG48G82G3C５ＣＦＵ／ｍＬG38G39G88。６．７ ５G87G67G5BG88G89G8AG85G7D６．７．１ G5EG5FG5AG60６．７．１．１ １０％（G7FG80G38G81）G67G8BG8CG5EG5FG23GDAGEEGA5１００ｍＬGBEG3AGD2GFFGA9GF4GB6，G84９００ｍＬGB8G37GA9G46G6BGE4G47，GC5G80０．２２μｍGE9GDFG28GEAGEBG3CGEA，G82G3BG3CG3DG3E。６．７．１．２ ５G87G67G5BG88G89G77G78G8DG8EG5EG5FG23GDAGB0GA5２０．０ｍｇ５GF3GF4GB7GF5GF6G22G23G21G6FG81１００ｍＬGAEGEEGC0，G80１０ｍＬ１０％GF4GB6GA9GAAG88GAAGB1，G66GAE，GE8GC9０．２０ｍｇ／ｍＬG28G22G23G9CGC1G88。６．７．１．３ １犿犿狅犾／犔G8FG6FG5EG5F，狆犎３．０GEEGA5０．０８３ｍＬGABGB4GBA（１２ｍｏｌ／Ｌ）GACGADG66GAEGCD１０００ｍＬ，G50G5CｐＨGCD３．０。６．７．１．４ １００犿犿狅犾／犔G90G91G63G74G5EG5F，狆犎１３．０G23GDAGB0GA5４．００ｇG27GC8G30GB9G35GFA，GAAG81１００ｍＬGBFG37GA9G2E，GE1GC3GC4GAFGA8G2FG3AG80GBFG37GA9G66GAEGCD１０００ｍＬ，G50G5CｐＨGCD１３．０。６．７．１．５ G77G78G92G93G5EG5FG70G3FG29GA5５GF3GF4GB7GF5GF6G22G23G9CGC1GAAG88５μＬ、１５μＬ、２５μＬ、４０μＬ、５０μＬ、１００μＬ、１ｍＬ、２ｍＬGAF１００ｍＬGAEGEEGC0G2E，G80１０％GF4GB6GA9GAAG88GACGADGAFG40GEA，GE8GC9０．０１μｇ／ｍＬ、０．０３μｇ／ｍＬ、０．０５μｇ／ｍＬ、０．０８μｇ／ｍＬ、０．１０μｇ／ｍＬ、０．２０μｇ／ｍＬ、１．００μｇ／ｍＬ、２．００μｇ／ｍＬG22G23G3EGD4GAAG88。GFEGE8GFEG80。６．７．２ G47G48G49G4AG38G39G5CG75G65６．１．１。G41G3AGA5G42G36G43１．００ｇG2FG36G68G69G6AG6BG6CG6DG6EG6FG30G81G44G5BG4EG45GABG4DGF8。G70G3FGA5１０ｍＬｐＨ３．０G7CｐＨ１３．０G28GAAG88G30G81G46GABG4DGF8。GA6G2EG4DGC1４０．０℃G79G88G85G2BG2C。７ｄG3A，GB4GC4G6CG38G88GA7G31G49G36G3EG28GABG4DGF8。GC4G6CG38G88G47G25GA7G48G49（６０．０℃，５０ｒ／ｍｉｎ），G66GAEGAF２ｍＬ，G43G8AG4AGFAGFB１２ｍｏｌ／ＬGB4GBA，１００．０℃GA9GB1１ｈ。G66GAEGAF５ｍＬ。G80０．４５μｍGEAGEBG3CGEA，G48G49GA6G2EGE1G74G88。６．７．３ G47G48G44G36GE5G4BG88GA1GBEG3AG79G88：GBEG3AG84G83G4CＣ１８，５μｍ，２５０ｍｍ×４．６ｍｍ（GF8GDF）。GE6GEBGA1G8B１０％GF4GB6GA9GAAG88。７犌犅／犜３８１７１—２０１９GE6GE7１．０ｍＬ／ｍｉｎ。G73G74G4DG4E２８５ｎｍ。G84G2F３０．０℃。G5FGA6GEE１０μＬ。G55GC4GDBGE5G4BG88GA1GBEG3AG79G88G89G22G23G3EGD4GAAG88G7CGA6G2EGE1G74G88G5FG71G73G74。G9DG9EG22G23G3EGD4GAAG88G28G44GFDG98G4FG55GCEG6FGD2GFB，G55G6FGD2GFBG89GA1G8AGABGEAG50G8DG22G23G3EGD4GFAGF5。G55G22G23G3EGD4GAAG88G28G44GFDG98G4FG89GA6G2EG5FG71G66GD9，G35G9DG9EG85G9CG44GFDG98G4FGF3G6FG28GD2GFB，G80G22G23G3EGD4GFAGF5G89GA6G2EG5FG71G66GEE。６．７．４ G4DG4EG4FG50G24G6E（７）G72G73：犡＝犆犞犿×１．４…………………………（７）G6EG2E：犡———G23G24G25G6EG6FG2E５GF3GF4GB7GF5GF6G28GF7GF0GEE，G38G39GCDG42GD8G23G24G25（μｇ／ｍＬ）；犆———G2DG3EGD4GFAGF5G72G48G28GABGA6GAAG88G2E５GF3GF4GB7GF5GF6G28GABGEA，G38G39GCDG42GD8G23G24G25（μｇ／ｍＬ）；犞———GABGA6G47GB4GBAGA9GB1G3AG97GDDG28G66GAEGFAGFB，G38G39GCDG24G25（ｍＬ）；犿———GB0GA5G28G68G69G6AG6BG6CG6DG6EG6FG28G6FGEE，G38G39GCDGD8（ｇ）；１．４———G68G69G6AG6BG6CG6DG6EG6FG6FGEEGA7G30GCDGFAGFBG28GA2G73G4AGF2。GC1G77G78GD9G79G88G85G7AG48G28GBFGBDG7BG7CG74G66G7DG7EG28G7FG89G80G81G8DG48G82G3CG73G45GE3GE4G81G28１０％。７ G43G94G2DG95７．１ G96G97G65GCAG3EG51G52G92G82G83，G6FGEEGE4GCAG28G83G2EGCDGCAG53。７．２ G98G47G24ＧＢ／Ｔ５４７５G28G29G66G5FG71。７．３ G99G9AG43G94G23G53G83G2EG27G54G55G8AG5FG71G73G76，G73G76G6BGAAG28G83G2EG5CG8EG27G54。G27G54G73G76GDBGDCGCDG56５G57G2EG29G66G28GDEGDF、G97GE5GE6GE7、GE8GB7GE9GEA、GEBGECGEDGEEG7CGEFGF0GF1GF2。７．４ G9BG9CG43G94７．４．１ G58G59G82G83G98，G23G5AGB1G8AG5FG71GCAGBDGCEG6EG73G76，G48G85G86G5BG5CGFEGCAG98G8AG5FG71GCEG6EG73G76：ａ）G98G83G2EGABG8DG5DG66G98；ｂ）G58G59G82G83G3A，G6AG5EG4C、G3EG51、G66GC1G48G5FG53GD1G30，G8EG60G60G61G83G2EGD9G60G98；ｃ）G83G2EG62G83G5AGB1G55GC4G63G78G82G83G98；ｄ）G27G54G73G76G7DG7EG84GC4GBDGCEG6EG73G76G48G5FG53G80G64G98；ｅ）GF7G65G66G67G34G27G4DG72G98。７．４．２ GCEG6EG73G76GDBGDCGCDG56５G57G2EG29G66G28G3FG48GDBGDC。７．５ G9DG36G2DG95７．５．１ G99G9AG43G94G9DG36G35G9EG43７．５．１．１ G27G54G73G76GDBGDCGDAG6B７．３G2EGDBGDCG4DG72，G68G66G21G53GCDG6BGAAG2E。７．５．１．２ G27G54G73G76GDBGDC１～２GDBG8DGDAG6BG4DG72，G8AG78G73，G78G73G3AG6AG69G48１GDBG8DGDAG6BG4DG72，G2AG68G66G9CG53GCDG8DG6B８犌犅／犜３８１７１—２０１９GAAG2E。７．５．１．３ G27G54G73G76GDBGDCG82G3C２GDBG8DGDAG6BG4DG72，G68G66G9CG53G83G2EGCDG8DG6BGAAG2E。７．５．２ G9BG9CG43G94G9DG36G35G9EG43７．５．２．１ GCEG6EG73G76GDBGDCGDAG6B７．４G2